Dipartimento di Geoscienze Università di Padova, Italy

The occurrence of crystallized and glassy melt inclusions (MI) in high-grade, partially melted metapelites and metagraywackes has opened up new possibilities to investigate anatectic processes. The present study focuses on three case studies: khondalites from the Kerala Khondalite Belt (India), the Ronda migmatites (Spain), and the Barun Gneiss (Nepal Himalaya). The results of a detailed microstructural investigation are reported, along with some new microchemical data on the bulk composition of MI. These inclusions were trapped within peritectic garnet and ilmenite during crystal growth and are therefore primary inclusions. They are generally isometric and very small in size, mostly £15 lm, and only rarely reaching 30 lm; they occur in clusters. In most cases inclusions are crystallized ( nanogranites ) and contain a granitic phase assemblage with quartz, feldspar and one or two mica depending on the particular case study, commonly with accessory phases (mainly zircon, apatite, rutile). In many cases the polycrystalline aggregates that make up the nanogranites show igneous microstructures, e.g. granophyric intergrowths, micrographic quartz in K-feldspar and cuneiform rods of quartz in plagioclase. Further evidence for the former presence of melt within the investigated inclusions consists of melt pseudomorphs, similar to those recognized at larger scale in the host migmatites. Moreover, partially crystallized inclusions are locally abundant and together with very small (£8 lm) glassy inclusions may occur in the same clusters. Both crystallized and partially crystallized inclusions often display a diffuse nanoporosity, which may contain fluids, depending on the case study. After entrapment, inclusions underwent limited microstructural modifications, such as shape maturation, local necking down processes, and decrepitation (mainly in the Barun Gneiss), which did not influence their bulk composition. Re-homogenized nanogranites and glassy inclusions show a leucogranitic and peraluminous composition, consistent with the results of partial melting experiments on metapelites and metagraywackes. Anatectic MI should therefore be considered as a new and important opportunity to understand the partial melting processes.

Using as a case study a granulite from the Kerala Khondalite Belt, India, we show that a former anatectic melt can be preserved as tiny (<25 μm) droplets within refractory minerals,in this case garnet. The melt is either fully crystallized as a Qtz-Ab-Kfs-Bt cryptocrystalline aggregate (“nanogranite”), or completely glassy in inclusions <15 μm. Both nanogranite and glassy inclusions have a peraluminous, ultrapotassic granitic composition that, in this case, does not correspond to a “minimum melt” and points to high melting temperatures, in agreement with the ultrahigh-temperature origin of the rock. This discovery indicates that peritectic minerals, growing during incongruent melting reactions, act as hosts for inclusions of anatectic melt, and that in the general case of slow cooling of the crust these inclusions will occur as nanogranite. Exceptionally, in the smallest inclusions, glass may be present due to inhibition of crystallization. Our results extend the frontiers of petrological and geochemical research in crustal melting, as the composition of natural anatectic melts can be directly analyzed rather than assumed.